October 17th, 2014 : 1014-175 : Enthalpy Analytical (Courtesy of FlavourCrafters)

17 October 2014 (1014-175)

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These test results have been provided as a courtesy by FlavourCrafters.

They contain results of three liquids that we currently carry and those flavours have been  highlighted  within the summary pages.

We are unable to provide this report in its entirety since it is not our report. Please contact them directly if you wish to obtain the entire report.

Flavour Blueberry
2.4%
Vanilla Cake
2.4%
Coconut Cream Pie
2.4%
Sample ID ECTA002-032 ECTA002-034 ECTA002-038
Enthalpy Code 1014-175-01 1014-175-03 1014-175-07
Nicotine Concentration
MDL: 0.100 mg/ml
24.0 mg/ml 24.8 mg/ml 22.8 mg/ml
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.286 µg/ml
1.09 J µg/ml 6.62 µg/ml ND
Acetoin
MDL: 0.923 µg/ml
ND 216 µg/ml ND
Diacetyl
MDL: 0.279 µg/ml
ND 10.6 µg/ml 92.5 µg/ml
See Actions
Formaldehyde
MDL: 0.846 µg/ml
1.31 µg/ml 1.23 µg/ml 2.75 µg/ml
Pentanedione
MDL: 0.281 µg/ml
ND 32.0 µg/ml 18.5 µg/ml
pH 9.36 8.37 8.24
% Water 1.83% 0.55% 5.47%
Flavour Honey Dew Melon
2.4%
Double Double Coffee
1.8%
Full Flavour Tobacco
1.8%
Sample ID ECTA002-039 ECTA002-041 ECTA002-042
Enthalpy Code 1014-175-08 1014-175-10 1014-175-11
Nicotine Concentration
MDL: 0.100 mg/ml
23.3 mg/ml 17.2 mg/ml 18.0 mg/ml
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.286 µg/ml
ND 1.87 J µg/ml 2.56 µg/ml
Acetoin
MDL: 0.923 µg/ml
ND 85.1 µg/ml ND
Diacetyl
MDL: 0.279 µg/ml
ND 10.6 µg/ml ND
Formaldehyde
MDL: 0.846 µg/ml
1.88 µg/ml 2.17 µg/ml 1.24 µg/ml
Pentanedione
MDL: 0.281 µg/ml
ND ND ND
pH 8.97 8.77 8.55
% Water 4.50% 2.04% 0.00%
Flavour Green Apple
1.8%
Coconut Tobacco
1.8%
Surf's Up
1.8%
Sample ID ECTA002-044 ECTA002-045 ECTA002-046
Enthalpy Code 1014-175-13 1014-175-14 1014-175-15
Nicotine Concentration
MDL: 0.100 mg/ml
18.5 mg/ml 17.1 mg/ml 17.3 mg/ml
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.286 µg/ml
0.951 J µg/ml 3.94 µg/ml 2.02 J µg/ml
Acetoin
MDL: 0.923 µg/ml
21.4 µg/ml 32.7 µg/ml 4.84 µg/ml
Diacetyl
MDL: 0.279 µg/ml
ND 3.58 µg/ml ND
Formaldehyde
MDL: 0.846 µg/ml
1.26 µg/ml 2.27 µg/ml 1.86 µg/ml
Pentanedione
MDL: 0.281 µg/ml
ND ND ND
pH 9.03 8.68 8.43
% Water 0.33% 0.66% 4.74%
Flavour Creamy Blueberry
1.8%
Lemonade
1.2%
Chocolate Hazelnut
1.2%
Sample ID ECTA002-047 ECTA002-049 ECTA002-050
Enthalpy Code 1014-175-16 1014-175-18 1014-175-19
Nicotine Concentration
MDL: 0.100 mg/ml
17.1 mg/ml 11.7 mg/ml 11.5 mg/ml
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.286 µg/ml
2.40 µg/ml 0.761 J µg/ml ND
Acetoin
MDL: 0.923 µg/ml
70.3 µg/ml 4.10 µg/ml 50.3 µg/ml
Diacetyl
MDL: 0.279 µg/ml
6.43 µg/ml ND 2.89 µg/ml
Formaldehyde
MDL: 0.846 µg/ml
2.29 µg/ml 3.27 µg/ml 1.80 µg/ml
Pentanedione
MDL: 0.281 µg/ml
6.38 µg/ml ND 10.8 µg/ml
pH 8.27 9.15 7.89
% Water 5.59% 0.54% 1.67%
Flavour Spearmint
1.2%
RY4
1.2%
Strawberry Shortcake
1.2%
Sample ID ECTA002-051 ECTA002-053 ECTA002-054
Enthalpy Code 1014-175-20 1014-175-22 1014-175-23
Nicotine Concentration
MDL: 0.100 mg/ml
11.6 mg/ml 11.6 mg/ml 11.3 mg/ml
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.286 µg/ml
1.37 J µg/ml 3.69 µg/ml 2.18 J µg/ml
Acetoin
MDL: 0.923 µg/ml
1.58 J µg/ml 2.44 J µg/ml 73.3 µg/ml
Diacetyl
MDL: 0.279 µg/ml
8.62 µg/ml ND 2.30 J µg/ml
Formaldehyde
MDL: 0.846 µg/ml
2.33 µg/ml 0.271 J µg/ml 3.45 µg/ml
Pentanedione
MDL: 0.281 µg/ml
ND ND 31.0 µg/ml
pH 8.94 8.35 7.62
% Water 0.57% 1.36% 5.43%
Flavour Belgian Elephant
1.2%
Funky Monkey
0.8%
Sour Black Raspberry
0.8%
Sample ID ECTA002-055 ECTA002-062 ECTA002-063
Enthalpy Code 1014-175-24 1014-175-31 1014-175-31
Nicotine Concentration
MDL: 0.100 mg/ml
11.5 mg/ml 7.51 mg/ml 7.06 mg/ml
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.286 µg/ml
1.36 J µg/ml 9.77 µg/ml 4.95 µg/ml
Acetoin
MDL: 0.923 µg/ml
55.0 µg/ml 3,278 µg/ml 19.8 µg/ml
Diacetyl
MDL: 0.279 µg/ml
2.26 J µg/ml 67.1 µg/ml
See Actions
ND
Formaldehyde
MDL: 0.846 µg/ml
1.58 µg/ml 4.14 µg/ml 2.43 µg/ml
Pentanedione
MDL: 0.281 µg/ml
6.21 µg/ml ND 4.33 µg/ml
pH 8.83 8.08 4.05
% Water 5.85% 4.60% 4.79%
Flavour Groovy Grape
Non-Nic
Ragin' Raspberry
Non-Nic
Red Energy Drink
Non-Nic
Sample ID ECTA002-067 ECTA002-068 ECTA002-070
Enthalpy Code 1014-175-36 1014-175-37 1014-175-39
Nicotine Concentration
MDL: 0.100 mg/ml
ND ND 12.3 mg/ml
See Actions
Diethylene glycol (DEG)
MDL: 2.23 µg/ml
ND ND ND
Acetaldehyde
MDL: 0.286 µg/ml
ND 13.4 µg/ml 0.823 J µg/ml
Acetoin
MDL: 0.923 µg/ml
1.83 J µg/ml 1.56 J µg/ml 2.53 J µg/ml
Diacetyl
MDL: 0.279 µg/ml
106 µg/ml
See Actions
RETESTED HERE
ND ND
Formaldehyde
MDL: 0.846 µg/ml
0.474 µg/ml 0.209 J µg/ml 1.72 µg/ml
Pentanedione
MDL: 0.281 µg/ml
ND ND ND
pH 4.41 3.95 8.86
% Water 0.46% 0.49% 1.43%

ND: Non Detect or analytical result below the MDL.
J: Results flagged "J" are below the Lower Curve Limit, above the MDL, and are considered estimates.

ACTIONS TAKEN:

  • Coconut Cream Pie, Diacetyl Detection more than 22 ppm - The manufacturer believes this could be coming from one of the flavourings and will work to eliminate the cause.
  • Funky Monkey, Diacetyl Detection more than 22 ppm - The manufacturer believes this could be coming from the Acetoin. They will to work to identify and eliminate the cause.
  • Groovy Grape, Diacetyl Detection more than 100 ppm - Immediate Stop Sale initiated. The manufacturer believes this could be coming from some sort of cross contamination. They will work to identify the issue and retest. RETESTED CLICK HERE
  • Red Energy Drink, Nicotine Level outside of ± 10% Range - The manufacturer indicates that this batch was never distributed. They have identified the issue as incorrect labelling and are reviewing their procedures to prevent future occurrences of this issue.

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The pages of the report showing these results are below:

Cover Page Report Page 4 Report Page 5
Report Page 6 Report Page 7 Report Page 8
Report Page 9 Report Page 10 Report Page 11
Report Page 12 Report Page 13 Report Page 14
Report Page 15 Report Page 16 Report Page 17
Report Page 24 Report Page 25 Report Page 26

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